Equipment Laboratory

Seven hoods and one hood suitable for synthesis with inert gas extinguishing system are available

Organic Analysis

maXis 3G and maXis II UHR-QTOF-MS, Bruker, both ultra high resolution quadrupole time-of-flight mass spectrometer, resolution 1 ppm, MS/MS and pseudo MS3 experiments, aquisition rate 50 Hz, electro spray ionization (ESI) source for coupling with LC, atmospheric pressure laser ionization (APLI) source for coupling with GC or LC, potentially feasible atmospheric pressure chemical ionization (APCI) source for coupling with GC or LC and atmospheric pressure photo ionization (APPI) source for coupling with GC or LC

GC-2010Plus (GC), Shimadzu, two split/splittless injectors SPL-2010plus, AOC20i autosampler, sample tray for 98 2 ml vials, two flowlines, flame ionization detector (FID), GCsolution software

Prominence UFLCXR (LC), Shimadzu, ultra performance liquid chromatography, 2 LC-20ADXR double plunger pumps, semi micro mixer, automatic rinsing kit, DGU-20A3 online degasser, SIL-20AXR autosampler, CTO-20AC column oven, SPD-20AV UV-detector, CBM-20A system controller, LC solution software

GCMS-QP-2010Plus EI/CI/NCI-System (GC-MS), Shimadzu, Optic3-PTV injector (split/splitless, programmed temperature vaporizer, on-column-injection, thermodesorption, difficult matrix introduction, rapid large volume injection) with LN2 cooling, additional split/splittless injector, Zoex modulator GCxGC with compressor cooling, Combi PAL Autosampler (liquid and headspace injection, automatized solid phase micro extraction, Peltier cooler 4°C to 70°C), simultaneous SIM and SCAN, GCMSsolution software, GC Image software, Cycle Composer software

TOC-L CPN, Shimadzu, TOC-/TIC-/TC-analyzer, ASI-L autosampler for 40 mL vials with magnetic stirrer and sparge option, suspended sample kit for measuring solids as suspensions, high salt sample combustion tube with additional halogen scrubber

SpeedExtractor E-916, Büchi, solvent extractor, parallel extraction of max. 6 samples, 12 stainless steel cells 10 ml and 6 stainless steel cells 40 ml, 250 ml collection vessels, possibility to use Büchi Syncore Analyst R-12 evaporation vessels as collection vessels

Syncore Analyst R-12, Büchi, parallel evaporation of 12 samples (120 ml) with residual volume cooling (0,3 ml), condenser, flushback module, solid phase extraction module, separate vacuum pump V-700 with controller V-855, rotation speed controlled

A 6 x 100, Seif Aufschlusstechnik, digestion apparatus for 6 x 100 mg samples, PTFE digestion vessels with quartz glass tubes, used in an oven

Hei-Vap Precision ML/HB/G3B, Heidolph, rotary evaporator, Rotavac vario control vacuum pump, AUTOaccurate temperature sensor

Vapotherm Basis Mobil I, Barkey, parallel evaporation of 10 samples (10 ml), max. set temperature 120 °C, viewing window (glass), turn over device, nitrogen gassing

Inorganic Analysis

ICP-OES SPECTROBLUE TI, SPECTRO Analytical Instruments, inductively coupled plasma optical emission spectrometry, Twin Interface for simultaneously axial and radial view on plasma (EOP+SOP), Teledyne CETAC ASX-560 autosampler, ICP Analyzer Pro software

761 Compact IC, Metrohm, ion chromatography, 753 supressor module, 813 Compact autosampler (36 samples), 761 Compact IC 1.1 software

Hydraulic and Soil Mechanic Laboratory

Pulverisette 7, Fritsch, planetary micro mill, 2 grinding beakers 12 ml and 45 ml stainless steel, (agate), silicium nitride each

Other Equipment

Genesys 10UV, Thermo, UV Vis spectrophotometer, Xenon lamp, 190 - 1100 nm

877 Titrino plus and 804 Ti Stand, Metrohm, for titration and constant pH, up to 20 ml

Alpha 1-4 LDplus, Christ, freezing dry machine, 0.51 kW, ice condenser temperature -60 °C, ice condenser chamber 6.5 l, 5 shelves á 360 mm diameter, 18 connections for round bottom flasks

Heraeus Multifuge X3 R, Thermo Fisher Scientific, up tp 18,517 x g, coolable -10°C - +40°C, 4 x Ø 100 mm, 6 x Ø 62 mm (250 mL) with 6 x high strength PTFE tubes usable to 18,517 x g

Biofuge R15, Heraeus, max. 20,000 x g, 24 x Ø 10 mm

SM 30 A, Edmund Bühler, shaker, orbital, up to 300 rpm

Milli-Q Integral 5, Millipore, ultrapure water purification system, TOC Analyzer, Q-POD Dispenser, PE Reservoir 30 l, typical electrical conductivity 0,055 µS/cm, typical TOC-concentration 3 ppb